دانلود کتاب Industrial Crystallization Process Monitoring and Control

Crystallization is an important technique for separation and purification of substances as well as for product design in chemical, pharmaceutical and biotechnological process industries. This ready reference and handbook draws on research work and industrial practice of a large group of experts in the various areas of industrial crystallization processes, capturing the essence of current trends, the markets, design tools and technologies in this key field. Along the way, it outlines trouble free production, provides laboratory controls, analyses case studies and discusses new challenges.First the instrumentation and techniques used to measure the crystal size distribution, the nucleation and solubility points, and the chemical composition of the solid and liquid phase are outlined. Then the main techniques adopted to control industrial crystallizers, starting from fundamental approaches to the most advanced ones, including the multivariable predictive control are described. An overview of the main crystallizer types is given with details of the main control schemes adopted in industry as well as the more suitable sensors and actuators.Content: Chapter 1 Characterization of Crystal Size Distribution (pages 1–6): Prof. Dr. Ing. Angelo ChianeseChapter 2 Forward Light Scattering (pages 7–20): Prof. Dr. Herman J. M. KramerChapter 3 Focused Beam Reflectance Measurement (pages 21–28): Jochen Scholl, Michel Kempkes and Marco MazzottiChapter 4 Turbidimetry for the Estimation of Crystal Average Size (pages 29–34): Prof. Dr. Ing. Angelo Chianese, Mariapaola Parisi and Eugenio FazioChapter 5 Imaging (pages 35–50): Prof. Dr. Herman J. M. Kramer and Somnath S. KadamChapter 6 Turbidimetry and Nephelometry (pages 51–57): Prof. Dr. Ing. Angelo Chianese, Marco Bravi and Eugenio FazioChapter 7 Speed of Sound (pages 59–69): Joachim Ulrich and Matthew J. JonesChapter 8 In?Line Process Refractometer for Concentration Measurement in Sugar Crystallizers (pages 71–79): Klas MyreenChapter 9 ATR?FTIR Spectroscopy (pages 81–91): Christian Lindenberg, Jeroen Cornel, Jochen Scholl and Marco MazzottiChapter 10 Raman Spectroscopy (pages 93–103): Jeroen Cornel, Christian Lindenberg, Jochen Scholl and Marco MazzottiChapter 11 Basic Recipe Control (pages 105–125): Alex N. Kalbasenka, Adrie E. M. Huesman and Prof. Dr. Herman J. M. KramerChapter 12 Seeding Technique in Batch Crystallization (pages 127–138): Joachim Ulrich and Matthew J. JonesChapter 13 Advanced Recipe Control (pages 139–159): Alex N. Kalbasenka, Adrie E. M. Huesman and Prof. Dr. Herman J. M. KramerChapter 14 Advanced Model?Based Recipe Control (pages 161–174): Alex N. Kalbasenka, Adrie E. M. Huesman and Prof. Dr. Herman J. M. KramerChapter 15 Fines Removal (pages 175–184): Prof. Dr. Ing. Angelo ChianeseChapter 16 Model Predictive Control (pages 185–201): Alex N. Kalbasenka, Adrie E. M. Huesman and Prof. Dr. Herman J. M. KramerChapter 17 Industrial Crystallizers Design and Control (pages 203–224): Franco Paroli